Titanium(II) chloride

Titanium(II) Chloride

Titanium(II) chloride

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Titanium(II) chloride is the chemical compound with the formula TiCl<sub>2</sub>. The black solid has been studied only moderately, probably because of its high reactivity.. The usual preparation is the thermal disproportionation of TiCl<sub>3</sub> at 500 °C. The equilibrium is "driven" by the loss of volatile TiCl<sub>4</sub>:
:2 TiCl<sub>3</sub> → TiCl<sub>2</sub> + TiCl<sub>4</sub>
The method is similar to that for the conversion of VCl<sub>3</sub> into VCl<sub>2</sub> and VCl<sub>4</sub>.

TiCl<sub>2</sub> crystallizes as the layered CdI<sub>2</sub> structure. Thus, the Ti(II) centers are octahedrally coordinated to six chloride ligands.


Molecular complexes are known such as TiCl<sub>2</sub>(chel)<sub>2</sub>, where chel is DMPE ((CH<sub>3</sub>)<sub>2</sub>PCH<sub>2</sub>CH<sub>2</sub>P(CH<sub>3</sub>)<sub>2</sub> and TMEDA...
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